US20210323294A1
2021-10-21
17/365,858
2021-07-01
A novel engineered wood product and method of making same that withstands the stresses, both natural and man-made, that cause warp, twist and bow.
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B32B37/1292 » CPC main
Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by using adhesives; Application of adhesive selectively, e.g. in stripes, in patterns
B32B21/10 » CPC further
Layered products comprising a layer of wood, e.g. wood board, veneer, wood particle board Next to a fibrous or filamentary layer
B32B38/0004 » CPC further
Ancillary operations in connection with laminating processes Cutting, tearing or severing, e.g. bursting; Cutter details
B32B38/0012 » CPC further
Ancillary operations in connection with laminating processes Mechanical treatment, e.g. roughening, deforming, stretching
C09J2400/14 » CPC further
Presence of inorganic and organic materials; Presence of inorganic materials Glass
B32B2037/1261 » CPC further
Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by using adhesives curable adhesive moisture curable
B32B2038/0056 » CPC further
Ancillary operations in connection with laminating processes; Other operations not otherwise provided for Moistening
C09J2475/00 » CPC further
Presence of polyurethane
B32B2313/04 » CPC further
Elements other than metals Carbon
B32B2317/16 » CPC further
Animal or vegetable based Wood, e.g. woodboard, fibreboard, woodchips
C09J2301/408 » CPC further
Additional features of adhesives in the form of films or foils characterized by the presence of essential components additives as essential feature of the adhesive layer
C09J2400/306 » CPC further
Presence of inorganic and organic materials; Presence of organic materials; Presence of wood in the pretreated surface to be joined
C09J2301/306 » CPC further
Additional features of adhesives in the form of films or foils characterized by the chemical, physicochemical or physical properties of the adhesive or the carrier the adhesive being water-activatable
B32B2375/00 » CPC further
Polyureas; Polyurethanes
B32B2038/0076 » CPC further
Ancillary operations in connection with laminating processes; Other operations not otherwise provided for Curing, vulcanising, cross-linking
B32B2315/085 » CPC further
Other materials containing non-metallic inorganic compounds not provided for in groups - ; Glass Glass fiber cloth or fabric
B32B37/12 IPC
Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by using adhesives
C09J7/32 » CPC further
Adhesives in the form of films or foils characterised by the adhesive composition Water-activated adhesive , e.g. for gummed paper
C09J5/02 » CPC further
Adhesive processes in general; Adhesive processes not provided for elsewhere, e.g. relating to primers involving pretreatment of the surfaces to be joined
C09J7/10 » CPC further
Adhesives in the form of films or foils without carriers
B32B38/08 » CPC further
Ancillary operations in connection with laminating processes Impregnating
B32B37/10 » CPC further
Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the pressing technique, e.g. using action of vacuum or fluid pressure
B32B38/00 IPC
Ancillary operations in connection with laminating processes
C09J11/04 » CPC further
Features of adhesives not provided for in group , e.g. additives; Non-macromolecular additives inorganic
This application is a continuation of U.S. Nonprovisional patent application Ser. No. 16/945,690, filed on Jul. 31, 2020 and claims priority to U.S. Provisional Patent Application No. 62/880,924, filed Jul. 31, 2019, the entire contents of which are incorporated herein by reference.
The present invention is directed to a composite wood product configured for withstanding stresses that cause warp, twist and bow, for example, stresses experienced by doors located between the interior and exterior of buildings and, more particularly, to a method of adhering a first solid wood board to a second solid wood board.
The present invention is directed to a novel engineered wood product and method of making same that withstands the stresses, both natural and man-made, that cause warp, twist and bow. The stabilization method produces a wood product that is exceptionally strong in both shear strength and tensile strength. The wood products produced by this process withstand extreme temperature differentials between the “faces” of the wood, e.g., as experienced between an outside face and an interior face of an exterior door, and maintains its intended shape. The process may be used with any number of solid wood slabs, such as white oak, alder, mahogany and the like. The process is especially useful when applied to wood species that are difficult to use in construction due to the high potential for warp and twist. Thus, the present invention may be used to stabilize lumber species that are notorious for warp and twist, such as hickory and white Oak.
FIG. 1 is a perspective view of pressure chamber.
FIG. 2 is a sectional view of a first board and a second board illustrating a pitch side and an outer growth ring side of same.
FIG. 3 is a perspective view a warp bias fiberglass yarn and a pair of wooden boards.
FIG. 4 is a perspective view of a vacuum chamber containing warp bias fiberglass yarn coated in a polyurethane resin.
FIG. 5 is a perspective view of a nitrogen gas purge tank and vacuum pump that is operatively coupled to the vacuum chamber.
FIG. 6 is a perspective view of a wooden board with warp bias fiber yarn fully impregnated with resin.
FIG. 7A is a sectional view of warp bias fiberglass yarn fibers in their natural state illustrating that the fibers are loosely organized with air space between the fibers.
FIG. 7B is a sectional view of warp bias fiberglass yarn fibers in their natural state illustrating that the fibers are loosely organized with air space between the fibers.
FIG. 8 is a sectional view of warp bias fiberglass yarn in their natural state impregnated with polyurethane resin illustrating air trapped within the resin.
FIG. 9 is a sectional view of warp bias fiberglass yarn impregnated with polyurethane resin and compressed illustrating entrapped air inside the compressed fibers and resin.
FIG. 10 is a sectional view of warp bias fiberglass yarn impregnated with polyurethane resin under vacuum in accordance with the present invention illustrating no air trapped inside of the resin.
FIG. 11 is a sectional view of warp bias fiberglass yarn impregnated with polyurethane resin under vacuum in accordance with the present invention illustrating a reduced thickness of the yarn following compression.
FIG. 12 is a perspective view a warp bias fiberglass yarn and a pair of wooden boards.
FIG. 13 is a sectional view of a fire resistant engineered wood product made in accordance with the present invention.
FIG. 14 is a sectional view of a fire resistant engineered wood product made in accordance with the present invention.
FIG. 15 is a perspective view of a platen and press used to compress the warp bias fiberglass saturated with polyurethane resin between two wood boards.
FIGS. 16 through 18 illustrate a engineered composite wood product made in accordance with the method of the present invention.
FIG. 19 is a perspective view of warp bias fiberglass yarn impregnated with polyurethane resin illustrating in the white portions thereof air trapped inside of the yarn.
FIG. 20 is a perspective view of warp bias fiberglass yarn impregnated with polyurethane resin under vacuum in accordance with the present invention illustrating the removal of all air from inside of the yarn.
Components of Finished Product
The engineered composite wood product of the present invention includes:
The method of making the engineered composite wood product of the present invention requires the following equipment:
Process for Preparing the Wood Slabs or Boards
Process for Impregnating Warp Bias Fiberglass or Similar Reinforcing Fiber with PUR Resin
Polyurethane Resin (PUR) is the preferred adhesive due to its affinity to both wood and fiberglass. It shall be noted that other adhesives could be used with this process and could have equal or better results. Polyurethane resin was chosen because it was the best option available at the time of discovery. PUR requires H2O as a catalyst which is normally found in the ambient air and within the wood boards or slabs used in the present invention. Once PUR is exposed to its catalyst, it begins curing by cross linking polymer chains within the PUR. If the curing process takes place in an uncontrolled environment the molecular structure of the PUR begins to expand and molecules move farther apart. If the PUR is restricted from moisture, i.e., 99.99% free of H2O, then the curing process will not begin, and the PUR molecules are free to be moved around without any concern of premature curing and therefore premature expansion. Thus, the PUR must be stored and delivered in an oxygen free environment. A pressurized nitrogen bath can be used to deliver the PUR to the reinforcement material without premature curing.
According to the present invention the warp bias fiberglass is impregnated with PUR as follows:
Description of Glass Fiber Orientation, with and without Resin, Improper Impregnation and Proper Impregnation.
The glass fibers are cylindrical extrusions of glass with a diameter of less than 0.0003″ (about 10 times smaller than a human hair.) The glass fibers are grouped together into a yarn, which contains several hundred fibers. In its natural state, the fibers are loosely organized with air space between the fibers. See FIGS. 7A and 7B. The vacuum process facilitates the complete displacement of air with PUR resin. Incomplete vacuum impregnation results in the PUR trapping air inside the collection of fibers. In this scenario the PUR also adds to the overall thickness of the yarn. See FIG. 8. As depicted in FIG. 8, the purple is the PUR and the yellow represents entrapped air inside the group of fibers.
Referring to FIG. 9, prior to the PUR impregnated fiber being are compressed between the boards, as hereinafter described, the purple represents PUR and yellow the entrapped air inside the compressed fibers. PUR is highly water resistant, and also when the glue joint is under compression it becomes airtight as well. The PUR effectively seals the air inside the fibers which results in a weakened bond line, and therefore is not protected from warp and twist.
Importance of Complete Impregnation of Glass Fiber with PUR
It is crucial that complete impregnation of the reinforcing glass fiber be achieved. When this process is done as outlined above, each glass fiber is surrounded by PUR, and all of the air is displaced. Referring to FIGS. 10 and 11, this type of bond results in realignment of the glass fibers, from a random displacement to a consistent displacement, with PUR resin adhering each fiber together, and filling any void spaces with hard resin. In FIGS. 10 and 11, the white portions represent PUR completely surrounding fibers. When the process is completed as described, the result is a solid bond line that shrinks in overall thickness by about 0.0065″ after compression.
Pressing Process
If the wood preparation process, the impregnation process and the pressing process have been done correctly, there should be a thinning of the reinforcing fiber which is a result of the fibers realigning themselves with the flat referenced flat surfaces.
Fiber Characteristics Before and after Impregnation and Pressing
Warp-Bias Fiberglass (10.5 oz) was used in in the example of the present invention described above, although we found statistically similar relative results using woven carbon fiber; however, for the purpose of this description warp-bias fiberglass is the reference.
Final Product
Referring to FIGS. 16-18, the final product exhibits a near invisible bond line, many multiples stronger than native wood. The bond line can be placed in multiples in the wood piece, and mixed with fire retardant to accomplish fire ratings that were not possible with wood before. The line can be painted or stained so it can be used where a solid wood appearance aesthetic is sought.
Producing Fire Rated Wood Panels Using this Process
The method described above may be used to make fire-rated wood panels without the need to treat the wood in a separate process. In order to produce fire rated panels and/or lumber, one simply needs to add fire retardant to the PUR mixture in combination with the vacuum process described above. The addition of various concentrations of fire retardant is normally accomplished by the adhesive manufacturer in concert with a chemist. Once the PUR has fire retardant added, the process of impregnation of the fiber stays the same as mentioned above, however the placement of the impregnated fabric will change, as illustrated in FIG. 13.
Referring to FIGS. 13 and 14, there are two sacrificial pieces of wood veneer that are placed on the outer faces of the lumber/panel. The sacrificial pieces of veneer are designed to burn away in a fire, which will leave the fire resistant reinforced fiber mat to protect the core of the panel. When used in door construction, this process easily withstands the fire hose test that is required by most independent certifying labs. The fire protection that is provided is directional in nature, i.e. it protects the structural core from the fire. Wood is a natural thermal insulator due to its open cellular structure within its fibers. The process of reinforcing wood with Fire Retardant PUR through the vacuum process described above allows the wood to remain structurally intact in the event of a fire. The engineered product can be made to withstand fire from a single direction, i.e. as in the case of a fire rated exterior door; or multiple directions which would be useful in building fire rated interior doors.
1.-4. (canceled)
5. A method of making a wood product comprising:
providing a first board and a second board,
forming a flat surface on each of the first board and the second board by milling a first face of the first board and a first face of the second board,
providing a first strip of reinforcing fiber selected from the group consisting of warp bias fiberglass, carbon fiber and combinations thereof,
saturating the first strip with a polyurethane resin (PUR),
arranging the PUR saturated first strip between the first face of the first board and the first face of the second board, and
compressing the PUR saturated first strip between the first face of the first board and the first face of the second board to thereby forming the wood product.
6. The method of claim 5, wherein each of the first face of the first board and the first face of the second board is formed by an outer tree-ring side of the respective boards.
7. The method of claim 5, including adding a fire retardant preparation to the PUR.
8. The method of claim 5, wherein each of the first board and the second board has a moisture content of 5% to 9%.
9. The method of claim 5, including milling the first face of the first board and the first face of the second board to each have a flatness with a tolerance zone of +/−0.005 inches per 60 inches of length.
10. The method of claim 5, including saturating the first strip with the PUR by placing the first strip in a vacuum chamber, purging oxygen from the vacuum chamber by displacing the oxygen with nitrogen, creating a vacuum in the vacuum chamber, applying the PUR to the first strip and maintaining the vacuum for an amount of time sufficient to fully saturate the first strip with the PUR.
11. The method of claim 10, wherein each and every filament of the first strip is completely surrounded by the PUR.
12. The method of claim 10, wherein all voids in the strip are displaced by the PUR.
13. The method of claim 10, wherein the filaments that compose the first strip are realigned and a thickness of the first strip is decreased to an average thickness of about 0.0165 inches to an average thickness of about 0.0065 inches.
14. The method of claim 5, including providing a first veneer, a second veneer, a second strip reinforcing fiber and a third strip of reinforcing fiber, saturating the second strip and the third strip with PUR containing a fire retardant, and compressing the PUR saturated second strip between the a second face of the first board and the first veneer and the PUR saturated third strip between a second face of the second board and the second veneer to thereby form a fire retardant wood product.
15. The method of claim 5, including applying a mist of water to each of the first faces of the first and second boards prior to compressing the PUR saturated first strip between the first face of the first board and the first face of the second board.
16. A method of making a wood product comprising:
forming a flat surface on each of a first face of a first board and a first face of a second board,
providing a first strip of reinforcing fiber saturated with a polyurethane resin (PUR) selected from the group consisting of warp bias fiberglass, carbon fiber and combinations thereof, and
compressing the PUR saturated first strip between the first face of the first board and the first face of the second board to thereby forming the wood product.
17. The method of claim 16, wherein each of the first board and the second board has a moisture content of 5% to 9%.
18. The method of claim 16, including milling the first face of the first board and the first face of the second board to each have a flatness with a tolerance zone of +/−0.005 inches per 60 inches of length.
19. The method of claim 16, including saturating the first strip with the PUR by placing the first strip in a vacuum chamber, displacing oxygen in the vacuum chamber with nitrogen, creating a vacuum in the vacuum chamber, applying the PUR to the first strip and maintaining the vacuum for an amount of time sufficient to saturate the first strip with the PUR.
20. The method of claim 16, wherein each and every filament of the first strip is surrounded by the PUR.
21. The method of claim 16, wherein essentially all voids in the strip are displaced by the PUR.
22. The method of claim 16, wherein the filaments that compose the first strip are realigned and a thickness of the first strip is decreased to an average thickness of about 0.0165 inches to an average thickness of about 0.0065 inches.
23. The method of claim 16, including providing a first veneer, a second veneer, a second strip reinforcing fiber and a third strip of reinforcing fiber, saturating the second strip and the third strip with PUR, and compressing the PUR saturated second strip between the a second face of the first board and the first veneer and the PUR saturated third strip between a second face of the second board and the second veneer to thereby form the wood product.
24. The method of claim 16, including applying a mist of water to each of the first faces of the first and second boards prior to compressing the PUR saturated first strip between the first face of the first board and the first face of the second board.
25. A wood product prepared in accordance with the method of claim 16.